Thermal Analysis of Polymers, Chemia, Analiza termiczna DSC krystalizacja polimerów (Thermal analysis DSC ...
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THERMAL ANALYSIS OF
POLYMERS
THERMAL ANALYSIS OF
POLYMERS
Fundamentals and Applications
EDITED BY
JOSEPH D. MENCZEL
Alcon Laboratories
Fort Worth TX
R. BRUCE PRIME
San Jose, CA
A JOHN WILEY & SONS, INC., PUBLICATION
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Library of Congress Cataloging-in-Publication Data:
Thermal analysis of polymers: fundamentals and applications / edited by Joseph D. Menczel,
R. Bruce Prime.
p. cm
Includes bibliographical references and index.
ISBN 978-0-471-76917-0 (cloth)
1. Polymers–Analysis. 2. Thermal analysis. I. Menczel, Joseph D. II. Prime, R. Bruce.
QD139.P6.T4452008
547′.7046—dc22
2008024101
Printed in the United States of America
10 9 8 7 6 5 4 3 2 1
CONTENTS
PREFACE
ix
1 INTRODUCTION
1
Joseph D. Menczel, R. Bruce Prime and Patrick K. Gallagher
2 DIFFERENTIAL SCANNING CALORIMETRY (DSC)
7
Joseph D. Menczel, Lawrence Judovits, R. Bruce Prime,
Harvey E. Bair, Mike Reading, and Steven Swier
2.1. Introduction /
2.2. Elements of Thermodynamics in DSC /
2.3. The Basics of Differential Scanning Calorimetry /
2.4. Purity Determination of Low-Molecular-Mass Compounds by
DSC /
2.5. Calibration of Differential Scanning Calorimeters /
2.6. Measurement of Heat Capacity /
2.7. Phase Transitions in Amorphous and Crystalline Polymers /
2.8. Fibers /
2.9. Films /
2.10. Thermosets /
2.11. Differential Photocalorimetry (DPC) /
2.12. Fast-Scan DSC /
2.13. Modulated Temperature Differential Scanning Calorimetry
(MTDSC) /
2.14. How to Perform DSC Measurements /
2.15.
Instrumentation /
Appendix /
Abbreviations /
References /
v
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